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All Communication should be addressed to Head Sophisticated analytical Instrument, Facillity, CSIR-Central Drug Research Institute, Sector 10, Jankipuram Extension, Sitapur Road, Lucknow 226031, Uttar Pradesh, INDIA  
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Charges & Sample Requirement
S.No. Facility Requirements on Test Sample Charges in Rs./hr./sample/spectrum Service Tax (15%) will be extra
Industry Govt. institution  Academia/
University
1. 1.) JMS- T100LC, Accu TOF Mass Spectrometer
(DART-MS)

2.) Agilent 6520 Q-Tof (ESI-HRMS & APCI-HRMS)

3.) Waters UPLC- TQD (ESI-MS and APCI-MS)
Triple Quadrupole
(L C-MS/MS)
1 - 2 mg
Nature of the sample, solubility, melting point, elements present and expected molecular weight.


Note - ESI-HRMS & APCI- HRMS are possible only in methanol, acetonitrile or water.


5-10 mg sample, LC conditions & LC trace for LCMS and LC- MS/MS


Note -
ESI /APCI-MS, LCMS and LC-MS/MS are possible only in methanol, acetonitrile or water.
3000/-
DART-MS per sample.



6000/-
DART/ APCI/ESI HRMS analysis.


3000/-
ESI / APCI-MS analysis.

3000/- * *
LCMS and LC-MS/ MS per hr.
1350/-
 DART-MS per sample.



2700/-

DART/ APCI/ESI HRMS analysis.


1350/-
ESI / APCI-MS analysis.

1350/- * *
LCMS and LC-MS/ MS per hr.
450/-
DART-MS per sample.



900/-

DART/ APCI/ESI HRMS analysis.


450/-
ESI / APCI-MS analysis.

450/- * *
LCMS and LC-MS/ MS per hr.
2. FT-NMR Spectrometers

1.) Bruker AvIII HD-300 MHz FT NMR with low and high temperature facility -90°C to 80°C




2.) Bruker AvII- 400
MHz FT NMR with, 5 mm multi- nuclear Broad band inverse probe, VT facility and also with HRMAS accessory

3.) Agilent DD2-700
MHz Four channel NMR spectrometer, equipped with triple resonance-VT probe and 13C- enhanced cold probe.
2-4 mg for 1HNMR and 30-40 mg for 13CNMR experiment. Solubility and nature of compound, eg. carcinogenic,toxic,lachrymato ry,explosive,hygroscopic etc.,Structural formula (contemplated / known) to be mentioned. RADIOACTIVE MATERIAL should not be submitted. Required amount of sample must be soluble in 0.6 ml of deuterated solvent. Facilities available for multinuclear and 2Dimensional homo- and hetero nuclear (inverse detection) experiments as well.

For HRMAS measurements 100-500 μg sample must be soluble in 12-50 μl of solvent for 1HNMR, 2 mg soluble in 50 μl of solvent for 13C or inverse 2D experiments(1H-13C). Gel NMR measurement as well as resin bound molecules NMR measurement can be caried out



1-2 mm
concentration for 1H- NMR experiments, >10mM for heteronuclear experiments at natural abundance. For proteins, 1-2mM isotopically labelled 13C/15N) samples needed to be ( submitted for multi dimensional experiments.
2000/-
for each half hr.or less solvent charges 200/- extra for deuterated solvents other than CDCL3 and D2O.





2000/-
solvent charges 200/- extra for deuterated solvents other than CDCL3 and D2O.




6000/-
for each half hr.or less 200/- solvent charges extra for deuterated solvents other than CDCl3 and D2O.
900/-
for each half hr.or less solvent charges 200/-extra for deuterated solvents other than CDCL3 and D2O.





900/-
solvent charges 200/-extra for deuterated solvents other than CDCL3 and D2O.




2700/-
for each half hr.or less 200/- solvent charges extra for deuterated solvents other than CDCl3 and D2O.
300/-
for each half hr.or less solvent charges 200/- extra for deuterated solvents other than CDCL3 and D2O.





300/-
solvent charges 200/-extra for deuterated solvents other than CDCL3 and D2O.




900/-
for each half hr.or less 200/- solvent charges extra for deuterated solvents other than CDCl3 and D2O.
3. FT IR Spectrometer Perkin Elimer Spectrum II
(4000-400 cm-1 )
5-10 mg
KBr/Nujol/CsI/CHCL3, nature (hygroscopic,explosive,etc.)
1000/-
per spectrum per samples
450/-
per spectrum per samples
150/-
per spectrum per samples
4. Elemental Analyzers
Euro –E 3000
10 mg
Other elements present, approximate % of nitrogen
800/-
per element per sample (CHNS & O) - separate samples required for Oxygen analysis * Fluorine containing samples are not accepted
360/-
per element per sample (CHNS & O) - separate samples required for Oxygen analysis * Fluorine containing samples are not accepted
120/-
per element per sample (CHNS & O) - separate samples required for Oxygen analysis * Fluorine containing samples are not accepted
Charges given are for Private Industries.
National Laboratories and Private & Government Small Scale Industries .
Educational Institutions.
Discount charges are not applicable for the deuterated solvents.
Note-The above charges for acquiring and providing you the data, not for the analysis.  * * Additional charges for sample preparation (Rs.150/-) and data processing (Rs. 300/-) per sample.
Please Note :
As per Govt.rules Service Tax (15%) will be charged on the analysis charges.
The analytical data/spectra are provided only for research/development purposes. These can not be used as certificates in legal disputes.
Service charges are payable in advance by crossed bank draft in favour of the Director, Central Drug Research Institute, Lucknow-226031.
Samples and payment should be sent preferably in the same cover. Seperate samples should be sent for different analysis. Samples are not analysed till payment is received.
Maximum 5 samples per lot for any type of analysis are accepted at a time.
Please send the samples in quantity as mentioned in the brochure. Samples are not recovered unless a special request is made.
In all correspondence related to analysis our reference number must be mentioned.
Radio-active samples shall be accepted only after prior approval of HOD, SAIF and handed over personally with BARC certification for the lab & details about the radio activity.
Unstable and explosive compounds are not accepted for analysis.
Services are rendered to only those users who regularly give us feedback about the end-use of the results, e.g., thesis, patent, process, publication etc.
All concern persons, research fellows and students are advised to send their application and samples through their supervisors or Head of Department. The request should be made only on University/College/Institute letter head.
Interpretation of spectra is not undertaken normally. In special cases this service can be provided on payment of extra charges.
All Communications should be addressed to :
Head
Sophisticated Analytical Instrument Facility
Central Drug Research Institute
Sector 10, Jankipuram Extension, Sitapur Road, Post Box No. 173
Lucknow 226031, Uttar Pradesh, INDIA
 
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